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Fast Exchange Refrigerator for Neutron Science (FERNS)--Containerless Research, Inc., 906 University Place, Evanston, IL 60201-3147; 847-467-2678, www.containerless.com

Dr. Richard Weber, Principal Investigator, weber@containerless.com 

Mr. John Nordine, Business Official, jnordine@containerless.com

DOE Grant No. DE-FG02-03ER83633

Amount:  $731,744  

Next-generation high flux neutron sources, such as the Spallation Neutron Source (SNS) at Oak Ridge National Laboratory, will allow faster-than-ever data collection rates.  Unfortunately, the present generation of neutron sample environment equipment (cryostats, furnaces, etc.) lacks the automation features needed to handle the high demand by non-expert users for rapid experiments and frequent sample changes.  This project will develop and deliver an advanced automated, programmable sample handling system for use in cryogenic sample environments for neutron research.  The approach will integrate state-of-the-art cryogenic and computer-controlled automation technologies to create a “Fast Exchange Refrigerator for Neutron Sciences,” specifically designed to increase experimental throughput in the next-generation neutron user facilities.   The new facility will be targeted to high flux beamlines that will enable investigation of a large number of samples.  In Phase I, instrument requirements were determined through discussions with users, and a breadboard instrument, control software, and sample holders were constructed.  In tests using a cryostat, test samples were exchanged in less than one minute.  Cool-down tests indicated that pre-cooling of samples would not be required to achieve fast turnaround.  In Phase II, design parameters will be fixed; a prototype instrument will be constructed and fully documented; software will be prepared for use with ethernet-based control; simple, inexpensive sample encapsulation will be developed; and the instrument will be delivered, tested, and installed at an SNS beamline.

Commercial Applications and Other Benefits as described by awardee: The instrument should satisfy a need of emerging neutron scattering facilities, where there would be a market for partially automated facilities.  In addition to the target market in neutron instrumentation, a modified version of the instrument would serve markets in X-ray diffraction.