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High-Performance Plasticization-Resistant Membranes for Natural Gas Separations--Membrane Technology and Research, Inc., 1360 Willow Road, Suite 103, Menlo Park, CA  94025-1524; 650-328-2228, www.mtrinc.com 

Dr. Ingo Pinnau, Principal Investigator, ipin@mtrinc.com 

Ms. Elizabeth Weiss, Business Official, egweiss@mtrinc.com

DOE Grant No. DE-FG02-03ER83710

Amount:  $749,994

Approximately 20% of U.S. natural gas reserves are subquality due to a high carbon dioxide content.  Membrane separation is an attractive technology to remove this carbon dioxide; however, membranes with higher flux and selectivity are required to improve the economics and reliability of the technology.  This project will develop a new type of fluorinated polymer membrane that has exceptional permeation characteristics and is resistant to plasticization and attack by higher hydrocarbons, aromatics, and other liquids.  In Phase I, thin-film composite membranes were made from a series of glassy polymers that were chemically modified using a novel fluorination process.  The best membranes had carbon dioxide/methane selectivities of 35 to 40 and carbon dioxide permeances of 70 GPU when tested at 500 to 1,000 psi with hydrocarbon-rich gas.  In Phase II, these membranes will be scaled up to industrial scale and evaluated in pilot-scale systems at natural gas processing plants. 

Commercial Applications and Other Benefits as described by awardee:  Currently, membrane separation has only a 4-6% share of the total carbon dioxide/natural gas separation market.  Improved membranes should lower the cost of membrane processes and substantially increase the membrane market share.